The HI934 is a Karl Fischer coulometric titrator with high accuracy, great flexibility and repeatability.
The titrator is designed to perform titrations for a variety of applications, allowing the user to obtain both good results and high-speed analysis. The HI934 analyzes for water content ranging from 1 ppm to 5%. This powerful titrator effectively monitors the KF reaction, detects the endpoint, and performs all necessary calculations and graphing.
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Small footprint, requires minimal bench space
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Casing made with strong, chemically resistant plastic
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Powerful built-in algorithms for termination criteria based on fixed mV endpoint or absolute/relative drift
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Sample analysis averaging and statistical data
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Minimized water vapor entry with the sealed solvent system
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Balance interface for automatic weighing
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Support for 100 titration methods
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User-customizable reports
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Clearly displayed warning and error messages
Coulometric Reagent System
Precision Iodine Generation
Hanna's dosing algorithm allows for an extremely small amount
of iodine necessary for the Karl Fischer reaction to be generated
electrolytically using a pulsed current up to 400 mA delivering titrant
accurately and precisely.
Titration and Solvent System
Chemically Resistant Titration Vessel and Tubing
The glass titration cell and PTFE tubing is designed to withstand the
harsh solvents and reagents involved in Karl Fischer reactions.
Sealed Solvent System
Ground glass joints completely seal the glass titration cell minimizing
exposure to ambient humidity, keeping the system dry, and reducing
reagent consumption while saving time between titrations. Solvent
may be exchanged in a matter of seconds with a quick fitting adjustment.
Molecular Sieve Desiccant
High efficiency molecular sieve desiccant helps maintain low and
stable drift rates within the titration cell while preventing the ingress
of ambient humidity into the sealed solvent system.
Digital built-in stirrer
Automatic, integrated magnetic stirrer adjustable from 200-2000
RPM with optical feedback for automatic speed control.
Titrator Capabilities
Dynamic Titrant Dosing
The titration speed feature allows for timely and accurate titration
results by relating the amount of iodine generated to the mV response
from the Karl Fischer reaction.
Drift Rate Compensation
The HI934 automatically adjusts the titration calculation to account
for the effects of any ambient humidity entering the titration cell. This
provides a more accurate result by correcting for water not present in
the actual sample.
Titration Results Averaging
Successive results from a titration method may be averaged with
recording of the standard deviation.
Selectable Endpoint Criteria
The HI934 employs a dual platinum pin electrode for bivoltammetric
endpoint determination. Users may choose termination criteria based
on mV stability times or drift rates.
Multistage Cell Preparation
A pre-titration stage eliminates residual water present in the solvent
and the cell, providing a reliable baseline start to analysis. Standby
mode then keeps the solvent dry between titrations and when the
titrator is not in use.
Interface & Display
Detailed Titration Graphs
A real-time titration curve can be displayed during each titration; this
feature is useful when new methods are tested or when a procedure
requires optimization.
Interactive Color Display
A large, color LCD screen clearly shows the chosen titration method
along with results, units, drift rate, and mV value.
Simple and Quick Navigation
Virtual key selections present on the display allow for simple and quick
navigation between screens and menus without getting lost in a nest
of information.
Data & Storage
Customizable Titration Reports
Each titration report is fully customizable so users can ensure they are storing and filing the appropriate data required for their application and procedures.
Flexible GLP Management
All necessary GLP (Good Laboratory Practice) information can be recorded with each sample including: sample identification, company and operator name, date, time, electrode ID codes, and calibration information.
Effortless Data Transfer
Data can easily be transferred to a USB flash drive or PC with the Hanna HI900PC application software. The USB port allows for the transfer of titration methods, titration reports, and software upgrades via USB flash drive.
Methods of Analysis
Customizable Methods
The HI934 can store up to 100 user-defined or standard titration methods. Each method may be customized and optimized for performance based on application and user requirements.
Titration Method Support
Onsite installation, training, and customization is available from one of our Applications or Service experts. Hanna offers continued support via phone or webinar for any questions you might have along the way.
Adaptable Standard Methods
Our technical experts can program and customize standard methods developed by such affiliations as ISO, ASTM, AOAC, AOCS, EPA, and more directly onto your titrator. Ask our Sales Consultants which standard methods are possible with our HI934 Karl Fischer system.
Connectivity and Functionality
Configurable Balance Interface
Sample size may be automatically entered from any laboratory analytical balance with a RS232 serial output saving time and labor.
Multiple Peripherals
Users can print reports directly from the titrator using a standard parallel printer. An external monitor and keyboard may be attached for added versatility, as well as an analytical balance for automatic sample mass entry for titrations.
Versatile Data Management
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Easily incorporate into any existing GLP data management program:
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Easily record all necessary GLP information with every sample, such as sample identification, company and operator name, date, time, electrode ID codes and calibration information
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Data can be transferred to a PC using Hanna HI900PC software
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Easy transfer of methods, reports and software upgrades via a USB flash drive
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Users can print reports of analyses directly from the titrator using a standard parallel printer
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A keyboard can be attached for added versatility
Specifications
| Specification |
Detail |
| sku |
HI934 |
| Range |
1 ppm to 5% |
| Resolution |
0.1ppm to 0.0001% |
| Result Units |
%, ppm, ppt, mg/g, μg/g, mg, μg, mg/mL, μg/mL, mg Br/100g, g Br/100g, mg Br, g Br |
| Sample Type |
liquid or solid with external dissolution / extraction |
| Pre-Titration Conditioning |
automatic |
| Background Drift Correction |
automatic or user-selectable value |
| Endpoint Criteria |
fixed mV persistence, relative drift stop or absolute drift stop |
| Dosing |
dynamic |
| Result Statistics |
mean, standard deviation |
| Generator Configuration |
diaphragm or diaphragm-less |
| Generator Current Control |
automatic or fixed (400 mA) |
| Generator Type Detection |
automatic |
| Titration Vessel |
operating volume between 100 200 mL |
| Solvent Handling System |
Sealed system with integrated diaphragm air pump |
| Sensor Type |
HI76330 dual platinum pin polarization electrode |
| Sensor Connection |
BNC |
| Polarization Current |
1, 2, 5, or 10 μA |
| Voltage Range |
2 mV to 1100 mV |
| Voltage Resolution |
0.1 mV |
| Accuracy |
±0.1% |
| Programmable Stirrer |
magnetic, optically regulated, digital stirrer 200 to 2000 rpm resolution 100 rpm |
| Display |
5.7in. (320 x 240 pixel) color LCD |
| Methods |
up to 100 (standard and user) methods |
| Logging Data |
up to 100 complete titration reports and drift rate reports can be stored |
| Peripherals (Rear) |
PC Connection, USB Flash Drive, Analytical Balance, Printer, External PC Keyboard |
| GLP Conformity |
Good Laboratory Practice and instrument data storage and printing |
| Languages |
English, Portuguese. Spanish, and French |
| Enclosure Material |
ABS, PC and Stainless Steel |
| Keypad |
Polyester |
| Operating Environment |
10 to 40°C (50 to 104°F), up to 95% RH |
| Storage Environment |
-20 to 70°C (-4 to 158°F), up to 95% RH |
| Power Supply |
100-240 VAC -01 models, US plug (type A) -02 models, European plug (type C) |
| Dimensions |
315 x 205 x 375 mm (12.4 x 8.1 x 14.8 ) |
| Weight |
approx. 4.3 kg (9.5 lbs.) with 1 pump, stirrer and sensors |
| Warranty |
2 years |
Manuals
https://www.documentation.hannainst.com/manuals/preview/115
Ordering Info
HI934D-01 and HI934D-02 are supplied with diaphragm,
HI934-01 and HI934-02 are supplied without diaphragm
All Models Include: dual platinum pin electrode, air pump/stirrer assembly, titration vessel assembly (glass vessel, accessory port stopper, sample port cap and septum, stir bar, desiccant, desiccant cartridge, fittings), vessel support with adapter, pump locking screw with plastic
head, reagent bottle assembly (bottle cap, desiccant, desiccant cartridge, fittings, tubing (silicone and PTFE)), water bottle assembly (waste bottle, bottle cap, desiccant, desiccant cartridge, fittings, tubing (silicone and PTFE)), calibration key, reagent exchange adapter, accessory holder assembly, joint grease, Karl Fischer generator electrode (removable generator electrode cable), USB cable, USB storage device,
HI900 PC application software, power adapter, quality certificate and instruction manual binder.